Two–Dimensional NMR Methods for Establishing Molecular Connectivity – A Chemist′s Guide to Experiment Selection, Perform and Interpretation
A Chemist′s Guide to Experiment Selection, Performance, and Interpretation
Gebonden Engels 1988 9780471187073Samenvatting
This guide to two–dimensional NMR spectroscopy helps the novice who want e the technique, but needs a path through the bewildering array of metho acronyms and the mathematical rigor found in most books.
The authors provide a clear explanation of experiment performance, param lection, data processing and presentation as well as a description of wh rmation is provided by each experiment and how it is extracted and inter They group presentations of two–dimensional NMR experiments according t zation, e.g. COSY, LRCOSY, ZQCOSY, DQCOSY ... for establishing proton–pr nnectivities.
The book also presents spectra of the same model compound using various ues to enable the reader to make direct comparisons and facilitate his e nt selection. Examples of the concerted utilization of various two–dimen NMR experiments to solve complex structural problems are also given.
Specificaties
Lezersrecensies
Inhoudsopgave
<br />
<br /> Heteronuclear Chemical shift Correlation.
<br />
<br /> Relayed Coherence Transfer and Related 2D–NMR Experiments.
<br />
<br /> 13—C–13—C Double Coherence 2D–NMR. The Inadequate Experiments.
<br />
<br /> Applications Problems.
<br />
<br /> Solutions to Problems.
<br />
<br /> Index.
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